ORGLIST: about the synthesis of N-2-bromoethylphthalimide

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From: wpxyj$##$163.net
Date: Sat Jan 16 1999 - 06:59:07 EST


Sir:
   I want to synthesis N-2-bromoethylphthalimide. I followed this method: Organic Synthesis, Vol., 32, p.18. It's said in this method that after phosphrous tribromide was added, the mixture should be heated under reflux.
I couldn't understand this. Which can be refluxed under this condition. Can a heating mantle substituted for a steam bath?
   Thank you advanced.
   With kind regards,
                                          Yanjun Xing

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