RE: ORGLIST: help regarding deprotection of Amine group

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From: will jones (willjones46$##$hotmail.com)
Date: Fri Oct 14 2005 - 04:59:49 EDT


Have you tried TMSI/base hydrolysis?

If that doesnt work with your system, pick an amine protecting group that
is!!

A decent quick overview found here.

http://cook.chem.ndsu.nodak.edu/files/worms/050223-worms-grc-nprot.pdf

Will


>From: "Mr. (Dr.) Hardik M. Thakar" <hardikthakar$##$rediffmail.com>
>Reply-To: "Mr. (Dr.) Hardik M. Thakar" <hardikthakar$##$rediffmail.com>
>To: everybody$##$orglist.net
>Subject: ORGLIST: help regarding deprotection of Amine group
>Date: 13 Oct 2005 05:52:04 -0000
>
>  
>Dear All,
>
>I protected my amine group with ethyl carbamate (NHCOOEt) some body help me
>to deprotect it.
>
>Sincerely,
>
>Hardik Thakar
>
>Thakar Hardik M.
>Ph.D. Student,
>B V Patel PERD Centre,
>S G Road,
>Thaltej,
>Ahmedabad-380054,
>India.
>Mob. No. :-+91-9825877320
>Fax. +91-79-27450449


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